9C9D

Protein receptor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-09-19
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.953731000423
Spacegroup name	P 1 21 1
Unit cell lengths	83.292, 115.530, 92.404
Unit cell angles	90.00, 114.60, 90.00

Refinement procedure

Resolution	43.780 - 2.900
R-factor	0.1911
Rwork	0.190
R-free	0.21550
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.490
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHENIX
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	43.780	3.004
High resolution limit [Å]	2.900	2.900
Number of reflections	35257	3482
<I/σ(I)>	9.55
Completeness [%]	99.7
Redundancy	3.5
CC(1/2)	0.994	0.574

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	EVAPORATION		295	PEG 8K, (NH4)2SO4, MES