9C9C

Protein receptor

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	AUSTRALIAN SYNCHROTRON BEAMLINE MX2
Synchrotron site	Australian Synchrotron
Beamline	MX2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-10-05
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9537
Spacegroup name	P 2 21 21
Unit cell lengths	50.165, 63.056, 144.736
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.260 - 1.660
R-factor	0.1747
Rwork	0.174
R-free	0.19560
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.857
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHENIX
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.250	1.690
High resolution limit [Å]	1.660	1.660
Rmerge	0.059
Number of reflections	54877	2657
<I/σ(I)>	15.9
Completeness [%]	99.6
Redundancy	6.8
CC(1/2)		0.622

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	imidazole, peg