9BZC

Cocrystal structure of Clostridium beijerinckii ZTP riboswitch with ZMP and Cs

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-02-07
Detector	DECTRIS PILATUS 6M-F
Wavelength(s)	1.4938
Spacegroup name	C 1 2 1
Unit cell lengths	99.864, 47.673, 74.110
Unit cell angles	90.00, 129.26, 90.00

Refinement procedure

Resolution	49.860 - 2.520
R-factor	0.1983
Rwork	0.195
R-free	0.22550
Structure solution method	SAD
RMSD bond length	0.005
RMSD bond angle	0.948
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	AutoSol
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.860	2.620
High resolution limit [Å]	2.520	2.520
Number of reflections	17648	1756
<I/σ(I)>	9.1
Completeness [%]	97.2
Redundancy	3.5
CC(1/2)	0.985	0.846

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION		294