9BNA
RE-REFINEMENT OF THE B-DODECAMER D(CGCGAATTCGCG) WITH A COMPARATIVE ANALYSIS OF THE SOLVENT IN IT AND IN THE Z-HEXAMER D(5BRCG5BRCG5BRCG)
Experimental procedure
Detector technology | DIFFRACTOMETER |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 24.870, 40.390, 66.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 5.000 - 1.900 |
R-factor | 0.188 |
RMSD bond length | 0.012 |
RMSD bond angle | 0.026 |
Refinement software | NUCLSQ |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 8.000 |
High resolution limit [Å] | 1.900 |
Number of reflections | 5691 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7.5 * | 290 | Wing, R., (1980) Nature, 287, 755. * |
Crystallization Reagents
ID | crystal ID | solution ID | reagent name | concentration | details |
1 | 1 | 1 | WATER | ||
2 | 1 | 1 | MPD | ||
3 | 1 | 1 | MG ACETATE | ||
4 | 1 | 1 | SPERMINE_HCL |
Crystallization Reagents in Literatures
ID | crystal ID | solution | reagent name | concentration (unit) | details |
1 | 1 | drop | DNA | ||
2 | 1 | drop | magnesium acetate | ||
3 | 1 | drop | spermine hydrochloride molecule | ||
4 | 1 | reservoir | MPD | 20-30 (%) |