9B4V
4F-Trp labeled Oscillatoria Agardhii Agglutinin (OAA)
Spectrometer
Experimental method: SOLID-STATE NMR
| Spectrometer ID | Spectrometer maker | Spectrometer model | Spectrometer type | Spectrometer field strength |
| 1 | Bruker | AVANCE III | 850 | |
| 2 | Bruker | AVANCE III HD | 600 | |
| 3 | Bruker | AVANCE III | 500 |
Experiment
| experiment id | conditions id | solution id | Experiment type |
| 1 | 1 | 1 | 2D CORD 25 ms |
| 10 | 1 | 1 | 2D hCH HETCOR |
| 11 | 1 | 1 | 2D hNH HETCOR |
| 12 | 1 | 1 | 2D 19F-19F RFDR |
| 13 | 1 | 1 | 2D hCF HETCOR |
| 14 | 1 | 1 | 3D hCHF HETCOR |
| 2 | 1 | 1 | 2D CORD 50 ms |
| 3 | 1 | 1 | 2D CORD 100 ms |
| 4 | 1 | 1 | 2D CORD 250 ms |
| 5 | 1 | 1 | 2D CORD 500 ms |
| 6 | 1 | 1 | 2D NCACX 50 ms |
| 7 | 1 | 1 | 2D NCOCX 25 ms |
| 8 | 1 | 1 | 3D NCACX 50 ms |
| 9 | 1 | 1 | 3D NCOCX 25 ms |
NMR Sample
| conditions id | NMR sample pH | NMR sample pressure | NMR sample temperature |
| 1 | 6.3 | 1 | 298 |
Conformers
| Conformers Calculated Total Number | 1000 |
| Conformers Submitted Total Number | 10 |
