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9AY8

Structure of the A type blood alpha-D-galactosamine galactosaminidase from Flavonifractor plautii

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsCLSI BEAMLINE 08B1-1
Synchrotron siteCLSI
Beamline08B1-1
Temperature [K]100
Detector technologyPIXEL
Collection date2022-09-27
DetectorDECTRIS PILATUS3 S 6M
Wavelength(s)1.1806
Spacegroup nameP 1 21 1
Unit cell lengths102.685, 164.568, 131.645
Unit cell angles90.00, 90.30, 90.00
Refinement procedure
Resolution39.440 - 2.000
R-factor0.169
Rwork0.168
R-free0.19330
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.008
RMSD bond angle1.465
Data reduction softwareXDS
Data scaling softwareAimless
Phasing softwarePHASER
Refinement softwareREFMAC (5.8.0425)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]39.4402.030
High resolution limit [Å]2.0002.000
Rmerge0.0631.244
Rmeas0.0751.472
Rpim0.0400.781
Total number of observations48915
Number of reflections29023514258
<I/σ(I)>13.61
Completeness [%]98.9
Redundancy3.43.4
CC(1/2)0.9980.403
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP2920.1 M BICINE pH 9, 20% w/v PEG 6000

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