9AXB

Structure of Gp54 from Escherichia phage Bas11

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007
Temperature [K]	100
Detector technology	CCD
Collection date	2023-10-18
Detector	RIGAKU SATURN 944
Wavelength(s)	1.5406
Spacegroup name	P 1
Unit cell lengths	50.000, 54.630, 54.590
Unit cell angles	78.54, 78.83, 69.88

Refinement procedure

Resolution	24.290 - 2.300
R-factor	0.2151
Rwork	0.211
R-free	0.25180
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.478
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	24.290	24.290	2.110
High resolution limit [Å]	1.990	5.900	1.990
Rmerge	0.074	0.036	0.910
Rmeas	0.104	0.051	1.288
Number of reflections	26616	1259	1253
<I/σ(I)>	6.91
Completeness [%]	73.1
Redundancy	2
CC(1/2)	0.994	0.995	0.405

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	3.2 M potassium acetate pH 7.0