9SIZ

CK1d in complex with IG138

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-06-07
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 1 21 1
Unit cell lengths	48.950, 73.930, 89.530
Unit cell angles	90.00, 103.18, 90.00

Refinement procedure

Resolution	39.370 - 1.500
R-factor	0.1604
Rwork	0.159
R-free	0.18320
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.919
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.370	1.554
High resolution limit [Å]	1.500	1.500
Rpim	0.024
Number of reflections	93506	8988
<I/σ(I)>	17.51
Completeness [%]	94.1
Redundancy	2
CC(1/2)	0.999	0.875

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5	277.15	0.1 M Sodium Malonate, pH 5 15-22% PEG3350