9SIX

CK1d in complex with IG130

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 11.2C
Synchrotron site	ELETTRA
Beamline	11.2C
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-10-04
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 1 21 1
Unit cell lengths	48.900, 73.910, 89.120
Unit cell angles	90.00, 103.17, 90.00

Refinement procedure

Resolution	47.610 - 1.230
R-factor	0.1642
Rwork	0.163
R-free	0.17940
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.847
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.19.2_4158: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.610	1.270
High resolution limit [Å]	1.230	1.230
Rpim	0.022
Number of reflections	158677	14713
<I/σ(I)>	10.92
Completeness [%]	88.8
Redundancy	2
CC(1/2)	0.999	0.903

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP	5	277.15	0.1 M Sodium Malonate, pH 5 15-22% PEG3350