Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID30B |
| Synchrotron site | ESRF |
| Beamline | ID30B |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-07-07 |
| Detector | DECTRIS EIGER2 X 9M |
| Wavelength(s) | 0.976 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 143.290, 140.240, 88.800 |
| Unit cell angles | 90.00, 124.06, 90.00 |
Refinement procedure
| Resolution | 90.000 - 2.390 |
| R-factor | 0.223 |
| Rwork | 0.221 |
| R-free | 0.26300 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.190 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.7) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 90.600 | 2.430 |
| High resolution limit [Å] | 2.390 | 2.390 |
| Rmerge | 0.059 | 0.494 |
| Number of reflections | 56900 | 2862 |
| <I/σ(I)> | 11.9 | 2.2 |
| Completeness [%] | 99.9 | 99.9 |
| Redundancy | 4.2 | 4.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 298 | 2.5 M AMS 0.1 M Hepes pH 6.9-7.7 |
