Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-04-27 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0000 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 67.236, 100.946, 90.251 |
| Unit cell angles | 90.00, 108.12, 90.00 |
Refinement procedure
| Resolution | 54.050 - 1.890 |
| R-factor | 0.19032 |
| Rwork | 0.189 |
| R-free | 0.22702 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.443 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC ((Version 1.1.7)) |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 54.050 | 2.142 |
| High resolution limit [Å] | 1.890 | 1.894 |
| Rmerge | 0.071 | 1.210 |
| Rmeas | 0.063 | |
| Rpim | 0.038 | 0.611 |
| Number of reflections | 58473 | 2924 |
| <I/σ(I)> | 10 | 1.6 |
| Completeness [%] | 64.2 | 10.4 |
| Redundancy | 4.5 | 4.8 |
| CC(1/2) | 0.997 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 7 | 277 | isopropanol, imidazole |
