9P68

Crystal structure of hen egg white lysozyme at 300 Kelvin with Vaseline (Duplicate)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	BRUKER TURBO X-RAY SOURCE
Temperature [K]	300
Detector technology	PIXEL
Collection date	2024-07-01
Detector	Bruker PHOTON II
Wavelength(s)	1.54184
Spacegroup name	P 43 21 2
Unit cell lengths	79.226, 79.226, 38.047
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.011 - 1.499
Rwork	0.201
R-free	0.23580
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.761
Refinement software	REFMAC (5.8.0425)

Data quality characteristics

	Overall
Low resolution limit [Å]	28.011
High resolution limit [Å]	1.499
Number of reflections	19887
<I/σ(I)>	18
Completeness [%]	99.0
Redundancy	1
CC(1/2)	0.990

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		295	1.2 M NaCl and 100 mM AcONa pH 4.6