Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-10-14 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 92.559, 86.279, 90.972 |
| Unit cell angles | 90.00, 114.42, 90.00 |
Refinement procedure
| Resolution | 60.360 - 2.610 |
| R-factor | 0.21642 |
| Rwork | 0.215 |
| R-free | 0.24802 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 1.020 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | FFT |
| Refinement software | REFMAC (5.8.0430) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 60.360 | 2.850 |
| High resolution limit [Å] | 2.610 | 2.610 |
| Number of reflections | 12509 | 3353 |
| <I/σ(I)> | 7 | |
| Completeness [%] | 62.6 | |
| Redundancy | 4.1 | |
| CC(1/2) | 0.990 | 0.293 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | EVAPORATION | 291 | 0.2M tri-Sodium citrate 18 % w/v PEG 3,350 |
