9NEO

TEAD2 YAP binding domain (YBD)

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-2
Synchrotron site	SSRL
Beamline	BL9-2
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-10-02
Detector	DECTRIS PILATUS 6M
Wavelength(s)	1
Spacegroup name	C 1 2 1
Unit cell lengths	121.727, 61.691, 80.156
Unit cell angles	90.00, 117.26, 90.00

Refinement procedure

Resolution	57.640 - 3.130
R-factor	0.2505
Rwork	0.243
R-free	0.31640
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.017
RMSD bond angle	1.912
Data reduction software	xia2
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	57.640	3.400
High resolution limit [Å]	3.130	3.200
Number of reflections	15703	12000
<I/σ(I)>	2.3
Completeness [%]	90.6
Redundancy	3.5
CC(1/2)	0.800	0.200

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293.15	3.1M Na Formate, 100mM HEPES pH 7.5