9ND4

[0,8,11-2] Shifted tensegrity triangle with an (arm,center,arm) distribution of (0,8,11) base pairs and 2 nt sticky ends

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 17-ID
Synchrotron site	APS
Beamline	17-ID
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-11-13
Detector	DECTRIS EIGER X 9M
Wavelength(s)	1.000000
Spacegroup name	H 3
Unit cell lengths	98.097, 98.097, 116.395
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	39.900 - 5.300
R-factor	0.1261
Rwork	0.124
R-free	0.14520
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.006
RMSD bond angle	0.865
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	PHENIX (1.21.1_5286)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]	68.621	68.621	5.711
High resolution limit [Å]	5.300	10.447	5.301
Number of reflections	1412	202	203
<I/σ(I)>	13.3
Completeness [%]	93.2
Redundancy	10.5
CC(1/2)	0.999	0.999	0.083

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		293	100 mM MOPS, 1.25 M magnesium sulfate