9IRL

Crystal structure analysis of LW-Srci-2o in complex with c-Src.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL19U1
Synchrotron site	SSRF
Beamline	BL19U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-07-10
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97867
Spacegroup name	P 21 21 21
Unit cell lengths	51.114, 85.134, 107.361
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.408 - 2.031
R-factor	0.1894
Rwork	0.187
R-free	0.24320
Structure solution method	SIRAS
RMSD bond length	0.009
RMSD bond angle	1.015
Refinement software	PHENIX (1.12_2829)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.410	2.104
High resolution limit [Å]	2.031	2.031
Number of reflections	154158	2884
<I/σ(I)>	12.9
Completeness [%]	95.6
Redundancy	5.2
CC(1/2)	0.998	0.771

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		289	PEG 3350, Hepes 7.4