9INT
Crystal structure of the complex of the beta,kappa-carrageenase Cgbk16A from Wenyingzhuangia fucanilytica with an oligosaccharide of furcellaran
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-06-23 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.987 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 47.770, 76.930, 99.350 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.580 - 1.560 |
R-factor | 0.1588 |
Rwork | 0.158 |
R-free | 0.17710 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.023 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.580 | 1.620 |
High resolution limit [Å] | 1.560 | 1.560 |
Rmerge | 0.049 | |
Rmeas | 0.053 | |
Rpim | 0.020 | |
Number of reflections | 52972 | 51770 |
<I/σ(I)> | 27.9 | 5.5 |
Completeness [%] | 97.9 | 93.74 |
Redundancy | 12.7 | |
CC(1/2) | 1.000 | 0.963 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 290 | 25.5% PEG 4000, 15% Glycerol, 0.17 M Ammonium sulfate |