Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PETRA III, DESY BEAMLINE P11 |
| Synchrotron site | PETRA III, DESY |
| Beamline | P11 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-09-06 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.03321 |
| Spacegroup name | P 1 2 1 |
| Unit cell lengths | 158.340, 112.380, 177.940 |
| Unit cell angles | 90.00, 95.25, 90.00 |
Refinement procedure
| Resolution | 49.490 - 3.900 |
| R-factor | 0.26245 |
| Rwork | 0.259 |
| R-free | 0.33557 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.326 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.490 | 4.140 |
| High resolution limit [Å] | 3.900 | 3.900 |
| Number of reflections | 55075 | 8852 |
| <I/σ(I)> | 5.06 | 1.11 |
| Completeness [%] | 96.5 | 96.8 |
| Redundancy | 4.44 | |
| CC(1/2) | 0.978 | 0.483 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 292 | 0.2 M Sodium citrate, 0.1 M Bis-Tris propane pH 7.5, 20% w/v PEG 3350 |
