Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-11-24 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9998 |
| Spacegroup name | P 1 |
| Unit cell lengths | 88.799, 106.683, 121.143 |
| Unit cell angles | 65.05, 70.82, 76.58 |
Refinement procedure
| Resolution | 90.210 - 1.890 |
| R-factor | 0.16372 |
| Rwork | 0.163 |
| R-free | 0.20597 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 1.473 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC ((Version 1.1.7)) |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 90.210 | 1.930 |
| High resolution limit [Å] | 1.890 | 1.890 |
| Number of reflections | 289674 | 14469 |
| <I/σ(I)> | 5.3 | |
| Completeness [%] | 96.3 | |
| Redundancy | 2.2 | |
| CC(1/2) | 0.990 | 0.960 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 20% (w/v) PEG 2000 MME, 0.1M Tris pH 6.75 |
