9F99

Crystal structure of MUS81-EME1 bound by compound 10.

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SOLEIL BEAMLINE PROXIMA 1
Synchrotron site	SOLEIL
Beamline	PROXIMA 1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-04-05
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.97855
Spacegroup name	P 21 21 21
Unit cell lengths	111.348, 125.097, 218.005
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	38.946 - 2.803
R-factor	0.2421
Rwork	0.240
R-free	0.28040
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	0.930
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	BUSTER (2.11.8)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	38.946	3.113
High resolution limit [Å]	2.803	2.803
Number of reflections	38581	1930
<I/σ(I)>	10.7
Completeness [%]	94.8
Redundancy	6.7
CC(1/2)	0.999	0.946

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	15% ethanol