9EQH
WWP2 WW2-2,3-linker-HECT (WWP2-LH)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-04-24 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9795 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 44.009, 90.270, 111.177 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 70.079 - 2.050 |
Rwork | 0.213 |
R-free | 0.27490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 2.222 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 70.079 | 5.552 |
High resolution limit [Å] | 2.046 | 2.046 |
Rmerge | 0.190 | |
Rmeas | 0.205 | |
Rpim | 0.075 | |
Number of reflections | 28618 | 1419 |
<I/σ(I)> | 6.9 | |
Completeness [%] | 99.5 | 99.9 |
Redundancy | 6.7 | |
CC(1/2) | 0.994 | 0.486 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 289 | 100 mM MMT pH 6.0, 25 % PEG1500 |