9EN6
Crystal structure of RNA G2C4 repeats - native model pH 6.5
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, EMBL c/o DESY BEAMLINE P13 (MX1) |
Synchrotron site | PETRA III, EMBL c/o DESY |
Beamline | P13 (MX1) |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-03-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.72932 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 41.656, 45.840, 51.474 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.750 - 0.918 |
Rwork | 0.118 |
R-free | 0.12940 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 2.749 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 25.750 | 0.970 |
High resolution limit [Å] | 0.918 | 0.920 |
Number of reflections | 34769 | 5565 |
<I/σ(I)> | 17.2 | 1.59 |
Completeness [%] | 99.9 | 99.8 |
Redundancy | 13.3 | |
CC(1/2) | 0.990 | 0.730 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292 | 0.08M Magnesium acetate tetrahydrate, 0.05M Sodium cacodylate trihydrate pH 6.5, 30% v/w Polyethylene glycol 4,000 |