9EJV

Co-MAHF-9 A8R Metal Alpha-Helix Framework

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-08-30
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.688801
Spacegroup name	P 1
Unit cell lengths	9.682, 16.260, 24.696
Unit cell angles	99.61, 97.48, 107.03

Refinement procedure

Resolution	15.180 - 0.920
R-factor	0.1153
Rwork	0.113
R-free	0.13480
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.606
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	15.180	0.953
High resolution limit [Å]	0.920	0.920
Number of reflections	9050	928
<I/σ(I)>	9.9
Completeness [%]	93.4
Redundancy	3.5
CC(1/2)	0.998	0.710

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	water, acetonitrile, cobalt acetate, sodium hydroxide, methanol