9BJM
Crystal Structure of Inhibitor 5c in Complex with Prefusion RSV F Glycoprotein
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-08-20 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.000 |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 170.018, 170.018, 170.018 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.080 - 2.070 |
R-factor | 0.1855 |
Rwork | 0.185 |
R-free | 0.20310 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 0.934 |
Data reduction software | XDS (20210323) |
Data scaling software | XDS (20210323) |
Phasing software | PHASER (2.8.3) |
Refinement software | PHENIX (1.19.2_4158) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.080 | 2.144 |
High resolution limit [Å] | 2.070 | 2.070 |
Rpim | 0.052 | 0.450 |
Number of reflections | 51555 | 5080 |
<I/σ(I)> | 22.14 | 1.83 |
Completeness [%] | 100.0 | 100 |
Redundancy | 59.8 | 58.9 |
CC(1/2) | 0.999 | 0.733 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 3M NaFormate |