9BJM

Crystal Structure of Inhibitor 5c in Complex with Prefusion RSV F Glycoprotein

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2021-08-20
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.000
Spacegroup name	P 41 3 2
Unit cell lengths	170.018, 170.018, 170.018
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	49.080 - 2.070
R-factor	0.1855
Rwork	0.185
R-free	0.20310
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	0.934
Data reduction software	XDS (20210323)
Data scaling software	XDS (20210323)
Phasing software	PHASER (2.8.3)
Refinement software	PHENIX (1.19.2_4158)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	49.080	2.144
High resolution limit [Å]	2.070	2.070
Rpim	0.052	0.450
Number of reflections	51555	5080
<I/σ(I)>	22.14	1.83
Completeness [%]	100.0	100
Redundancy	59.8	58.9
CC(1/2)	0.999	0.733

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	3M NaFormate