9BBH
Co-crystal structure of human DDB1 bound to fragment UB028670
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU FR-E SUPERBRIGHT |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2021-09-14 |
Detector | RIGAKU SATURN A200 |
Wavelength(s) | 1.54 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 62.924, 125.268, 168.529 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.820 - 2.000 |
R-factor | 0.18992 |
Rwork | 0.188 |
R-free | 0.23191 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.135 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.820 | 2.030 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.110 | 0.819 |
Rmeas | 0.117 | 0.875 |
Rpim | 0.041 | 0.305 |
Total number of observations | 34490 | |
Number of reflections | 90240 | 4336 |
<I/σ(I)> | 16.7 | 2.7 |
Completeness [%] | 99.4 | |
Redundancy | 8 | 8 |
CC(1/2) | 0.999 | 0.751 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291 | 20% (v/w) PEG 3350, 0.2 M di-NH4tart |