9B75
Crystal structure of humanized 44H10 Fab Version 17
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 23-ID-D |
Synchrotron site | APS |
Beamline | 23-ID-D |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-02-11 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 1.0332 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 36.923, 84.844, 64.778 |
Unit cell angles | 90.00, 106.42, 90.00 |
Refinement procedure
Resolution | 35.420 - 1.950 |
R-factor | 0.1819 |
Rwork | 0.180 |
R-free | 0.22300 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.666 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 1.980 |
High resolution limit [Å] | 1.950 | 1.950 |
Number of reflections | 27394 | 1054 |
<I/σ(I)> | 8.6 | |
Completeness [%] | 97.9 | |
Redundancy | 3.4 | |
CC(1/2) | 0.993 | 0.763 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 20% PEG3350, 0.2 M potassium nitrate pH 6.9 |