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8ZM6

Crystal structure of Thermolysin (Dose III)

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsPAL/PLS BEAMLINE 11C
Synchrotron sitePAL/PLS
Beamline11C
Temperature [K]100
Detector technologyPIXEL
Collection date2022-05-04
DetectorDECTRIS PILATUS 6M
Wavelength(s)0.9794
Spacegroup nameP 61 2 2
Unit cell lengths93.141, 93.141, 128.777
Unit cell angles90.00, 90.00, 120.00
Refinement procedure
Resolution34.180 - 1.400
R-factor0.15238
Rwork0.152
R-free0.17244
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.012
RMSD bond angle1.758
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0415)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.370
High resolution limit [Å]1.3501.350
Number of reflections747933665
<I/σ(I)>32.89
Completeness [%]100.0
Redundancy32.6
CC(1/2)0.9960.703
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP293Tris, Ammonium sulfate

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