8Z53
Arabidopsis Dwarf14 (AtD14) co-crystallized in the presence of Zaxinone
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SOLEIL BEAMLINE PROXIMA 1 |
| Synchrotron site | SOLEIL |
| Beamline | PROXIMA 1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-09-26 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.988 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 43.820, 69.580, 89.860 |
| Unit cell angles | 90.00, 92.85, 90.00 |
Refinement procedure
| Resolution | 44.910 - 2.400 |
| R-factor | 0.18016 |
| Rwork | 0.178 |
| R-free | 0.22640 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | MOLREP |
| Refinement software | REFMAC (refmac5) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.910 | 2.480 |
| High resolution limit [Å] | 2.400 | 2.400 |
| Number of reflections | 20924 | 1788 |
| <I/σ(I)> | 17.77 | 2.77 |
| Completeness [%] | 98.5 | 90 |
| Redundancy | 6.6 | 4.6 |
| CC(1/2) | 0.999 | 0.850 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298 | 0.2 M Potassium sodium tartrate tetrahydrate, 20% w/v PEG 3350 |
