8YZT
Crystal structure of the BANP BEN domain in complex with its target DNA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 80 |
Detector technology | PIXEL |
Collection date | 2023-03-31 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97915 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 57.995, 58.060, 214.381 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 39.360 - 2.580 |
R-factor | 0.2289 |
Rwork | 0.225 |
R-free | 0.30460 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | AlphaFold |
RMSD bond length | 0.009 |
RMSD bond angle | 0.984 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHENIX |
Refinement software | PHENIX (1.13_2998) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.360 | 2.640 |
High resolution limit [Å] | 2.580 | 2.600 |
Rmerge | 0.139 | 0.591 |
Number of reflections | 23248 | 1109 |
<I/σ(I)> | 16.6 | |
Completeness [%] | 99.1 | |
Redundancy | 8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | containing 0.02 M citric acid, 0.08 M BIS-Tris propane (pH: 8.8) and 16% w/v polyethylene glycol 3,350 |