8YUN

The crystal structure of HNBP001-HCP

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-11-28
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.979
Spacegroup name	P 1
Unit cell lengths	82.077, 82.213, 100.116
Unit cell angles	89.99, 90.31, 119.73

Refinement procedure

Resolution	41.110 - 2.700
R-factor	0.2401
Rwork	0.228
R-free	0.26680
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.001
RMSD bond angle	0.377
Refinement software	PHENIX (1.18.2_3874)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	100.100	2.800
High resolution limit [Å]	2.683	2.700
Rmerge	0.109	0.638
Number of reflections	58085	58085
<I/σ(I)>	77.7
Completeness [%]	99.9
Redundancy	3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291.15	20% v/v 2-Propanol, 0.1 M Tris pH8.0, 5% w/v Polystyrene glycol 8,000