8YTQ
The structure of apoCopC from Thioalkalivibrio paradoxus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE MASSIF-3 |
Synchrotron site | ESRF |
Beamline | MASSIF-3 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-05-05 |
Detector | DECTRIS EIGER X 4M |
Wavelength(s) | 0.9677 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 28.084, 144.787, 55.350 |
Unit cell angles | 90.00, 90.07, 90.00 |
Refinement procedure
Resolution | 55.350 - 1.700 |
R-factor | 0.18644 |
Rwork | 0.184 |
R-free | 0.23063 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 2.155 |
Data reduction software | DIALS |
Data scaling software | Aimless |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 55.350 | 1.730 |
High resolution limit [Å] | 1.700 | 1.700 |
Rmerge | 0.086 | 0.612 |
Rmeas | 0.099 | 0.700 |
Rpim | 0.048 | 0.336 |
Total number of observations | 194184 | 10364 |
Number of reflections | 47498 | 2495 |
<I/σ(I)> | 7.7 | 1.8 |
Completeness [%] | 98.2 | |
Redundancy | 4.1 | 4.2 |
CC(1/2) | 0.995 | 0.814 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 288 | 0.1 M Sodium acetate trihydrate pH 4.6, 2.0 M Ammonium sulfate |