8YL9
Crystal structures of terpene synthases complexed with a substrate mimic
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL10U2 |
Synchrotron site | SSRF |
Beamline | BL10U2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-08-28 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97902 |
Spacegroup name | P 21 3 |
Unit cell lengths | 146.990, 146.990, 146.990 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 44.320 - 2.750 |
R-factor | 0.193 |
Rwork | 0.187 |
R-free | 0.26800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.222 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.320 | 2.900 |
High resolution limit [Å] | 2.750 | 2.750 |
Rmerge | 0.135 | 0.515 |
Number of reflections | 27686 | 3987 |
<I/σ(I)> | 27.8 | |
Completeness [%] | 99.6 | |
Redundancy | 36.7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 289 | 200 mM Magnesium formate and 26% w/v PEG3350 |