8YIK

pP1192R-ATPase-domain

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL17U1
Synchrotron site	SSRF
Beamline	BL17U1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2022-07-31
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.9790
Spacegroup name	P 61 2 2
Unit cell lengths	85.753, 85.753, 211.483
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	43.070 - 1.300
R-factor	0.2004
Rwork	0.200
R-free	0.20630
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	0.902
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	211.480	1.330
High resolution limit [Å]	1.300	1.300
Rmerge		0.092
Number of reflections	111723	1531
<I/σ(I)>	0
Completeness [%]	98.7
Redundancy	5
CC(1/2)	1.000

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		291	20%(W/V) PEG 3350