8YFZ
CRYSTAL STRUCTURE OF THE EST1 H274E MUTANT AT PH 4.2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 90 |
Detector technology | IMAGE PLATE |
Collection date | 2003-09-22 |
Detector | Bruker DIP-6040 |
Wavelength(s) | 0.9 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 58.522, 71.672, 136.840 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 18.340 - 1.500 |
R-factor | 0.167 |
Rwork | 0.166 |
R-free | 0.18400 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.355 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0005) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 18.600 | 1.580 |
High resolution limit [Å] | 1.500 | 1.500 |
Rmerge | 0.072 | 0.292 |
Number of reflections | 46125 | 46125 |
<I/σ(I)> | 10.9 | 2.6 |
Completeness [%] | 99.5 | 98.4 |
Redundancy | 3.9 | 2.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 4.2 | 293 | 12% PEG 3000, 200MM NACL, 100MM PHOSPHATE-CITRATE, PH 4.2, VAPOR DIFFUSION, TEMPERATURE 293K |