8YEY
TRIP4 ASCH domain in complex with ssDNA-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-03-15 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9792 |
Spacegroup name | P 1 2 1 |
Unit cell lengths | 38.077, 29.438, 126.462 |
Unit cell angles | 90.00, 89.91, 90.00 |
Refinement procedure
Resolution | 42.154 - 2.000 |
R-factor | 0.2042 |
Rwork | 0.201 |
R-free | 0.25810 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.929 |
Refinement software | PHENIX ((1.17.1_3660: ???)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.030 |
High resolution limit [Å] | 2.000 | 5.430 | 2.000 |
Rmerge | 0.119 | 0.089 | 0.430 |
Rmeas | 0.133 | 0.102 | 0.491 |
Rpim | 0.058 | 0.048 | 0.230 |
Total number of observations | 98282 | ||
Number of reflections | 19378 | 1040 | 869 |
<I/σ(I)> | 6.1 | ||
Completeness [%] | 99.0 | 97.9 | 92.9 |
Redundancy | 5.1 | 4.9 | 4.1 |
CC(1/2) | 1.000 | 0.987 | 0.799 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298.15 | 0.1 M Bicine (pH 8.5) and 20% (w/v) PEG 10,000 |