8Y7F

Crystal structure of CARF domain-truncated Csx1-Crn2 from Marinitoga sp.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRF BEAMLINE BL02U1
Synchrotron site	SSRF
Beamline	BL02U1
Temperature [K]	80
Detector technology	PIXEL
Collection date	2023-10-14
Detector	DECTRIS PILATUS 6M
Wavelength(s)	0.979
Spacegroup name	P 43 3 2
Unit cell lengths	210.580, 210.580, 210.580
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.530 - 2.950
R-factor	0.2014
Rwork	0.200
R-free	0.23020
Structure solution method	SAD
RMSD bond length	0.011
RMSD bond angle	1.301
Data reduction software	xia2
Data scaling software	xia2
Phasing software	PHENIX
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.530	3.060
High resolution limit [Å]	2.950	2.950
Number of reflections	34091	34091
<I/σ(I)>	19.7
Completeness [%]	100.0
Redundancy	39.7
CC(1/2)	0.999	1.000

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		298	0.2 M Calcium acetate,0.1 M Na cacodylate pH 6.5, 40% PEG 300