8Y6D
Norovirus GII.10 P domain and 2'-FL (tablet)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-11-02 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95372 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 65.408, 78.926, 70.074 |
Unit cell angles | 90.00, 101.13, 90.00 |
Refinement procedure
Resolution | 43.550 - 1.410 |
R-factor | 0.172 |
Rwork | 0.171 |
R-free | 0.19490 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.008 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHENIX |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.550 | 1.430 |
High resolution limit [Å] | 1.410 | 1.410 |
Rmerge | 0.060 | 1.261 |
Rmeas | 0.067 | 1.435 |
Rpim | 0.031 | 0.673 |
Total number of observations | 608864 | 26159 |
Number of reflections | 133866 | 6219 |
<I/σ(I)> | 9 | 0.7 |
Completeness [%] | 99.4 | |
Redundancy | 4.5 | 4.2 |
CC(1/2) | 0.998 | 0.506 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 300 | 0.2 M sodium nitrate 0.1 M bis-tris propane (pH 7.5) 20% (w/v) PEG3350 |