8Y6C
Norovirus GII.10 P domain and 2'-FL (powder)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-11-04 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.95365 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.988, 78.700, 70.770 |
Unit cell angles | 90.00, 102.83, 90.00 |
Refinement procedure
Resolution | 44.630 - 1.470 |
R-factor | 0.1678 |
Rwork | 0.167 |
R-free | 0.19060 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.004 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.630 | 1.490 |
High resolution limit [Å] | 1.470 | 1.470 |
Rmerge | 0.067 | 1.313 |
Rmeas | 0.075 | 1.494 |
Rpim | 0.035 | 0.702 |
Total number of observations | 556487 | 21864 |
Number of reflections | 122545 | 5094 |
<I/σ(I)> | 9.2 | 0.7 |
Completeness [%] | 99.0 | |
Redundancy | 4.5 | 4.3 |
CC(1/2) | 0.999 | 0.395 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 300 | 0.2 M sodium nitrate 0.1 M bis-tris propane (pH 7.5) 20% (w/v) PEG3350 |