8XQD
The Crystal Structure of PTPRG from Biortus.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | CLSI BEAMLINE 08ID-1 |
| Synchrotron site | CLSI |
| Beamline | 08ID-1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-08-13 |
| Detector | DECTRIS EIGER X 9M |
| Wavelength(s) | 1.18064 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 72.916, 76.161, 106.623 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 47.270 - 2.550 |
| R-factor | 0.2183 |
| Rwork | 0.215 |
| R-free | 0.27749 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.004 |
| RMSD bond angle | 1.015 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0411) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.270 | 2.660 |
| High resolution limit [Å] | 2.550 | 2.550 |
| Rmerge | 0.162 | 0.675 |
| Number of reflections | 20006 | 2394 |
| <I/σ(I)> | 9.3 | |
| Completeness [%] | 100.0 | |
| Redundancy | 7.2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.2M NaSCN, 20% PEG 3350 |
