8XPZ

The Crystal Structure of TTBK1 from Biortus.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	CLSI BEAMLINE 08ID-1
Synchrotron site	CLSI
Beamline	08ID-1
Temperature [K]	100
Detector technology	PIXEL
Collection date	2023-11-09
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.95355
Spacegroup name	C 1 2 1
Unit cell lengths	170.905, 40.204, 49.533
Unit cell angles	90.00, 103.72, 90.00

Refinement procedure

Resolution	48.165 - 2.600
Rwork	0.201
R-free	0.27330
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.336
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.165	2.720
High resolution limit [Å]	2.600	2.600
Rmerge	0.118	0.907
Number of reflections	10211	1215
<I/σ(I)>	8.4
Completeness [%]	99.0
Redundancy	5.2

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	0.5M LiCl, 0.1M Tris-HCl pH8.5, 28% PEG 6000