8X7X
Crystal structure of SADS-CoV fusion core
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 80 |
Detector technology | CCD |
Collection date | 2023-04-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 0.9785 |
Spacegroup name | H 3 2 |
Unit cell lengths | 45.176, 45.176, 418.012 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.560 - 2.590 |
R-factor | 0.2375 |
Rwork | 0.235 |
R-free | 0.28360 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 0.779 |
Data reduction software | HKL-3000 |
Data scaling software | HKL-3000 |
Phasing software | PHASER |
Refinement software | PHENIX ((1.17.1_3660: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 28.560 | 2.680 |
High resolution limit [Å] | 2.590 | 2.590 |
Number of reflections | 5590 | 55 |
<I/σ(I)> | 2 | |
Completeness [%] | 98.9 | |
Redundancy | 1 | |
CC(1/2) | 0.984 | 0.500 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 298 | 0.1M HEPES pH 7.5, 42% PEG 200 |