8X7C
Crystal structure of ZmHSL1A
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2023-06-20 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 1.06 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 88.062, 54.368, 174.744 |
| Unit cell angles | 90.00, 104.34, 90.00 |
Refinement procedure
| Resolution | 26.840 - 1.597 |
| R-factor | 0.175 |
| Rwork | 0.173 |
| R-free | 0.20370 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 0.814 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.13_2998: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.000 | 1.620 |
| High resolution limit [Å] | 1.597 | 1.600 |
| Rmerge | 0.042 | 0.374 |
| Number of reflections | 106167 | 3167 |
| <I/σ(I)> | 16.33 | 2.68 |
| Completeness [%] | 99.4 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.999 | 0.900 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | MES, PEG 4000 |
