8WZO
Parkin in complex with phospho NEDD8
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID30B |
Synchrotron site | ESRF |
Beamline | ID30B |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-09-28 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.8731 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 77.976, 47.747, 127.859 |
Unit cell angles | 90.00, 105.38, 90.00 |
Refinement procedure
Resolution | 40.947 - 2.250 |
Rwork | 0.207 |
R-free | 0.24850 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 5n2w |
RMSD bond length | 0.004 |
RMSD bond angle | 1.026 |
Data reduction software | xia2 |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0258) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 44.520 | 2.320 |
High resolution limit [Å] | 2.250 | 2.250 |
Number of reflections | 21772 | 1974 |
<I/σ(I)> | 8.4 | |
Completeness [%] | 99.8 | |
Redundancy | 4.3 | |
CC(1/2) | 0.993 | 0.643 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 277 | 0.02 M Sodium/potassium phosphate, 0.1 M Bis-Tris propane, 7.5, 20% w/v PEG 3350 |