8WXX
Structure of WDR5 in complex with WIN motif containing SET1B E1750R/G1751V
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2018-10-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9779 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 115.801, 47.244, 129.675 |
Unit cell angles | 90.00, 112.97, 90.00 |
Refinement procedure
Resolution | 27.210 - 2.100 |
R-factor | 0.1772 |
Rwork | 0.174 |
R-free | 0.21160 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.127 |
Data reduction software | HKL-2000 |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.095 | 0.474 |
Number of reflections | 37965 | 1855 |
<I/σ(I)> | 13.35 | |
Completeness [%] | 99.2 | |
Redundancy | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.5 | 291 | 0.1 M sodium citrate, pH 5.5, 16% PEG 4000, 10% 2-propanol |