8WW5
X-Ray crystal structure of glycoside hydrolase family 6 cellobiohydrolase from Phanerochaete chrysosporium PcCel6A C240S
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PHOTON FACTORY BEAMLINE BL-5A |
Synchrotron site | Photon Factory |
Beamline | BL-5A |
Temperature [K] | 95 |
Detector technology | PIXEL |
Collection date | 2022-12-01 |
Detector | DECTRIS PILATUS3 S 6M |
Wavelength(s) | 1.0000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 54.567, 67.368, 88.055 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.380 - 1.010 |
R-factor | 0.1473 |
Rwork | 0.147 |
R-free | 0.15390 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.833 |
Data reduction software | XDS |
Data scaling software | XDS |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.380 | 1.030 |
High resolution limit [Å] | 1.010 | 1.010 |
Rmerge | 0.055 | 1.127 |
Number of reflections | 169019 | 8050 |
<I/σ(I)> | 26.1 | 2.2 |
Completeness [%] | 99.4 | 97 |
Redundancy | 12.4 | 11.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5 | 293 | PEG 4000, sodium acetate, sodium chloride |