8WTK
Crystal structure of Cas3-DExD+MG
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | NSRRC BEAMLINE BL13B1 |
Synchrotron site | NSRRC |
Beamline | BL13B1 |
Temperature [K] | 293 |
Detector technology | CCD |
Collection date | 2020-01-01 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.0000 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 114.756, 114.756, 119.632 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 28.980 - 3.080 |
R-factor | 0.2286 |
Rwork | 0.224 |
R-free | 0.26950 |
Structure solution method | SAD |
RMSD bond length | 0.002 |
RMSD bond angle | 0.603 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.000 | 3.190 |
High resolution limit [Å] | 3.080 | 3.080 |
Number of reflections | 17162 | 1668 |
<I/σ(I)> | 6 | |
Completeness [%] | 99.5 | |
Redundancy | 5 | |
CC(1/2) | 0.850 | 0.850 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | EVAPORATION | 295.15 | 15% PEG3350, 10% glycerol, and 0.1 M Tris at a pH of 6.4 |