8WRF
Crystal structure of MexL
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL19U1 |
| Synchrotron site | SSRF |
| Beamline | BL19U1 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-04-24 |
| Detector | DECTRIS PILATUS3 6M |
| Wavelength(s) | 0.97861 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 103.090, 103.090, 146.640 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 32.960 - 3.000 |
| R-factor | 0.2121 |
| Rwork | 0.211 |
| R-free | 0.24180 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond angle | 4.941 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 32.960 | 3.000 |
| High resolution limit [Å] | 3.000 | 3.000 |
| Rmerge | 0.057 | |
| Rmeas | 0.058 | |
| Rpim | 0.013 | |
| Number of reflections | 18558 | 18558 |
| <I/σ(I)> | 43.86 | |
| Completeness [%] | 99.8 | |
| Redundancy | 19.3 | |
| CC(1/2) | 1.000 | 0.936 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 291 | 0.14 M K2HPO4, 1.26 M NaH2PO4 |
