8WFF
The Crystal Structure of LYN from Biortus.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-10-15 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.99999 |
Spacegroup name | P 61 |
Unit cell lengths | 45.730, 45.730, 56.686 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 39.603 - 1.300 |
Rwork | 0.155 |
R-free | 0.18220 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.011 |
RMSD bond angle | 1.569 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 39.603 | 1.320 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.078 | 0.293 |
Number of reflections | 16562 | 790 |
<I/σ(I)> | 19.2 | |
Completeness [%] | 99.7 | |
Redundancy | 9.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1M Citric acid pH3.5, 3.0M NaCl |