8WDI
Crystal structure of lysozyme by fixed-target pink-beam serial synchrotron crystallography
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 295 |
Detector technology | PIXEL |
Collection date | 2023-05-23 |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.8366 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.830, 78.830, 38.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 6.990 - 2.200 |
R-factor | 0.2561 |
Rwork | 0.251 |
R-free | 0.29930 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 0.969 |
Data reduction software | CrystFEL |
Data scaling software | CrystFEL |
Phasing software | MOLREP |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 79.360 | 2.270 |
High resolution limit [Å] | 2.200 | 2.200 |
Number of reflections | 6525 | 628 |
<I/σ(I)> | 5.43 | |
Completeness [%] | 100.0 | |
Redundancy | 492.9 | |
CC(1/2) | 0.874 | 0.524 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | SMALL TUBES | 295 | Na-acetate, NaCl, PEG8000 |