8WDG
Subatomic crystal structure of glucose isomerase from Streptomyces rubiginosus
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 11C |
Synchrotron site | PAL/PLS |
Beamline | 11C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-12-09 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.8265 |
Spacegroup name | I 2 2 2 |
Unit cell lengths | 92.675, 98.626, 102.137 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 40.770 - 0.990 |
R-factor | 0.15874 |
Rwork | 0.158 |
R-free | 0.17071 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.018 |
RMSD bond angle | 2.043 |
Data reduction software | xia2 |
Data scaling software | xia2 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.770 | 1.010 |
High resolution limit [Å] | 0.990 | 0.990 |
Number of reflections | 255970 | 12132 |
<I/σ(I)> | 12.2 | |
Completeness [%] | 99.5 | 94.6 |
Redundancy | 6.1 | |
CC(1/2) | 0.999 | 0.561 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 295 | Tris-HCl, pH 8.0, PEG400, MgCl2 |